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Sampling and Sample Preparation in Analytical Chemistry
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Authors: Jaroslava Švarc-Gajic (Bulevar cara Lazara 1, Faculty of Technology, Serbia) 
Book Description:
The art of sample manipulation considers adequate sample collection, preservation and storage, as well as its safe preparation. Analytical chemists often find themselves in a position to spend considerable more time and effort in preparing samples rather than analyzing them. In many cases the reliability of analysis is limited by the correctness of sample manipulation. The skills of sample manipulation are based on abundant knowledge, competence and rich experience. Being indispensable in every laboratory, educational or scientific institution, this book encompasses all relevant issues related to collecting samples of any kind, as well as methods of sample preparation for specific analytical goal. The presented material provides an overview of sampling principles and strategies supporting them with inevitable statistical background. (Imprint: Nova)

Table of Contents:
Introduction pp.1-2

Chapter I. Statistical Aspects in Analytical Chemistry pp.3-18

Chapter II. General Sampling Principles pp.19-22

Chapter III. Sampling Strategies pp.23-34

Chapter IV. Sample Size pp.35-38

Chapter V. Sample Collection pp.39-52

Chapter VI. Sample Storage and Preservation pp.53-62

Chapter VII. General Principles of Extraction pp.63-76

Chapter VIII. Membrane Extraction pp.77-84

Chapter IX. Extraction of Solids pp.85-104

Chapter X. Supercritical Fluid Extraction pp.105-112

Chapter XI. Subcritical Water Extraction pp.113-118

Chapter XII. Solid Phase Extraction pp.119-136

Chapter XIII. Quechers pp.137-140

Chapter XIV. Matrix Solid Phase Dispersion pp.141-142

Chapter XV. Solid Phase Microextraction pp.143-150

Chapter XVI. Sample Digestion pp.151-166

Chapter XVII. Dry Ashing pp.167-174

Chapter XVIII. Derivatization pp.175-190

Chapter XIX. Headspace Gas Chromatography pp.191-198

Chapter XX. Gel Permeation Chromatography pp.199-208

Chapter XXI. Measurement Uncertainty pp.209-228

Chapter XXII. Calculations in Sampling– Practical Examples pp.229-238

Chapter XXIII. Calculation of Measurement Uncertainty – Practical Examples pp.239-258

Appendix I, II, III pp.259-264

Index pp.265-277

      Chemistry Research and Applications
      Chemical Engineering Methods and Technology
   Binding: Hardcover
   Pub. Date: 2012 1st quarter
   Pages: 7 x 10 277.pp
   ISBN: 978-1-62100-269-7
   Status: AV
Status Code Description
AN Announcing
FM Formatting
PP Page Proofs
FP Final Production
EP Editorial Production
PR At Prepress
AP At Press
AV Available
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Sampling and Sample Preparation in Analytical Chemistry